Information card for entry 7017775

Structure parameters

• Formula: C36 H36 Cl8 N4 O2 Pd2
• Calculated formula: C36 H34.826 Cl8 N4 O2 Pd2
• Title of publication: A systematic study on the synthesis, reactivity and structure of ortho-palladated aryloximes, including the first cyclopalladated aryloximato and iminoaryloxime complexes.
• Authors of publication: Vicente, José; Chicote, María-Teresa; Abellán-López, Antonio; Bautista, Delia
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 3
• Pages of publication: 752 - 762
• a: 16.9138 ± 0.0006 Å
• b: 11.0175 ± 0.0004 Å
• c: 22.5029 ± 0.0009 Å
• α: 90°
• β: 90.541 ± 0.002°
• γ: 90°
• Cell volume: 4193.2 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.0885
• Weighted residual factors for all reflections included in the refinement: 0.0935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No