Information card for entry 7017852

Structure parameters

• Formula: C30 H57 Al2 Cl11 P4
• Calculated formula: C30 H57 Al2 Cl11 P4
• Title of publication: The relative stabilities of cyclic dicationic derivatives of diphosphanes with three (3P) or four (4P) linked phosphorus atoms.
• Authors of publication: Bashforth, Rachel; Boyall, Alice J.; Coffer, Philippa K.; Dillon, Keith B.; Goeta, Andrés E; Howard, Judith A. K.; Kenwright, Alan M.; Probert, Michael R.; Shepherd, Helena J.; Thompson, Amber L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 4
• Pages of publication: 1165 - 1172
• a: 38.5425 ± 0.0012 Å
• b: 11.8925 ± 0.0004 Å
• c: 26.5378 ± 0.0009 Å
• α: 90°
• β: 130.391 ± 0.001°
• γ: 90°
• Cell volume: 9264.6 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0882
• Weighted residual factors for all reflections included in the refinement: 0.0953
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No