Information card for entry 7018038

Structure parameters

• Formula: C32 H62 Co2 F12 N20 O28
• Calculated formula: C32 H62 Co2 F12 N20 O28
• Title of publication: Tetrapodal amidoxime ligands I. Coordination isomerism due to self-complementary dimerization of a pyramidal cobalt(iii) coordination module.
• Authors of publication: Boyd, John P.; Irran, Elisabeth; Grohmann, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 8
• Pages of publication: 2477 - 2485
• a: 9.2213 ± 0.0004 Å
• b: 12.9948 ± 0.0006 Å
• c: 13.4621 ± 0.0008 Å
• α: 69.118 ± 0.005°
• β: 83.997 ± 0.004°
• γ: 73.435 ± 0.004°
• Cell volume: 1444.63 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0534
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.0892
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 0.973
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No