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Information card for entry 7018141
Preview
Coordinates | 7018141.cif |
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Original paper (by DOI) | HTML |
Formula | As4 H140 K20 Mo6 O198 Pd2 S8 W36 |
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Calculated formula | As4 K10 Mo6 O178 Pd2 S8 W36 |
Title of publication | {AsW(9)O(33)}-{Mo(3)S(4)} based polyoxometalates including a metal-metal bond with Pd or Ni. Synthesis, structure and studies in solution. |
Authors of publication | Duval, Sylvain; Marrot, Jérôme; Simonnet-Jégat, Corine; Mbomekallé, Israël Martyr; Sokolov, Maxim; Cadot, Emmanuel |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2012 |
Journal volume | 41 |
Journal issue | 11 |
Pages of publication | 3174 - 3184 |
a | 16.3278 ± 0.0007 Å |
b | 18.5432 ± 0.0006 Å |
c | 20.1322 ± 0.0008 Å |
α | 71.099 ± 0.002° |
β | 73.208 ± 0.002° |
γ | 75.25 ± 0.002° |
Cell volume | 5432.9 ± 0.4 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1308 |
Residual factor for significantly intense reflections | 0.0815 |
Weighted residual factors for significantly intense reflections | 0.2077 |
Weighted residual factors for all reflections included in the refinement | 0.2643 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.092 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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