Information card for entry 7018690

Structure parameters

• Formula: C99 H78 Ga2 N12
• Calculated formula: C99 H78 Ga2 N12
• Title of publication: Diastereoselective generation of triple-stranded helicates induced by gem-dimethyl groups on a linker.
• Authors of publication: Zhang, Zhan; Chen, Yakun; Dolphin, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 16
• Pages of publication: 4751 - 4753
• a: 28.13 ± 0.0007 Å
• b: 12.85 ± 0.0003 Å
• c: 24.134 ± 0.0005 Å
• α: 90°
• β: 94.951 ± 0.001°
• γ: 90°
• Cell volume: 8691.2 ± 0.3 ų
• Cell temperature: 103 ± 0.1 K
• Ambient diffraction temperature: 103 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.0421
• Weighted residual factors for significantly intense reflections: 0.1057
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.105
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No