Information card for entry 7018722

Structure parameters

• Formula: C16 H6 Cl2 F12 Si
• Calculated formula: C16 H6 Cl2 F12 Si
• Title of publication: Synthesis and characterisation of selected group 14 derivatives of the 2,5-(CF(3))(2)C(6)H(3) (Ar) ligand.
• Authors of publication: Coffer, Philippa K.; Dillon, Keith B.; Howard, Judith A. K.; Yufit, Dmitry S.; Zorina, Natalia V.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 15
• Pages of publication: 4460 - 4468
• a: 19.4317 ± 0.0008 Å
• b: 17.0627 ± 0.0007 Å
• c: 22.8784 ± 0.0009 Å
• α: 90°
• β: 102.013 ± 0.001°
• γ: 90°
• Cell volume: 7419.4 ± 0.5 ų
• Cell temperature: 40 K
• Ambient diffraction temperature: 40 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0504
• Residual factor for significantly intense reflections: 0.0427
• Weighted residual factors for significantly intense reflections: 0.0984
• Weighted residual factors for all reflections included in the refinement: 0.1019
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No