Information card for entry 7018738

Structure parameters

• Formula: C182 H280 Cl2 Cu9 N18 O96
• Calculated formula: C182 H162 Cl2 Cu9 N18 O40
• Title of publication: Phase transfer catalyst supported, room-temperature biphasic synthesis: a facile approach to the synthesis of coordination polymers.
• Authors of publication: Zhao, Xiao-Liang; Sun, Di; Hu, Tuo-Ping; Yuan, Shuai; Gu, Li-Chuan; Cong, Heng-Jiang; He, Hai-Yan; Sun, Dao-Feng
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 15
• Pages of publication: 4320 - 4323
• a: 31.01 ± 0.004 Å
• b: 31.01 ± 0.004 Å
• c: 28.765 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 27661 ± 8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0846
• Residual factor for significantly intense reflections: 0.0801
• Weighted residual factors for significantly intense reflections: 0.2281
• Weighted residual factors for all reflections included in the refinement: 0.2348
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No