Information card for entry 7018911

Structure parameters

• Formula: C78 H66 Ag2 O7 P4
• Calculated formula: C78 H66 Ag2 O7 P4
• Title of publication: Mechanochemical and solution synthesis, and crystal structures and IR and solid-state (CPMAS) NMR spectroscopy of some bis(triphenylphosphine)silver(i) mono- and di-hydrogencitrate systems.
• Authors of publication: Bowmaker, Graham A.; Hanna, John V.; Skelton, Brian W.; White, Allan H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 17
• Pages of publication: 5409 - 5417
• a: 24.568 ± 0.002 Å
• b: 12.4749 ± 0.0007 Å
• c: 23.1076 ± 0.001 Å
• α: 90°
• β: 106.704 ± 0.006°
• γ: 90°
• Cell volume: 6783.2 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1776
• Residual factor for significantly intense reflections: 0.1271
• Weighted residual factors for significantly intense reflections: 0.3289
• Weighted residual factors for all reflections included in the refinement: 0.3519
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No