Information card for entry 7018923

Structure parameters

• Formula: C12 H60 Cu4 Ge Mo9 N12 O38
• Calculated formula: C12 H48 Cu4 Ge Mo9 N12 O38
• Title of publication: Four di-Cu(II)-substituted sandwich-type germanomolybdates obtained under different reaction conditions: from zero-dimensional to two-dimensional structure.
• Authors of publication: Li, Suzhi; Guo, Yuan Yuan; Zhang, Dongdi; Ma, Pengtao; Qiu, Xiaoyang; Wang, Jingping; Niu, Jingyang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 17
• Pages of publication: 5235 - 5240
• a: 13.0503 ± 0.0014 Å
• b: 14.0662 ± 0.0015 Å
• c: 17.4386 ± 0.0019 Å
• α: 79.75 ± 0.002°
• β: 73.805 ± 0.002°
• γ: 64.567 ± 0.002°
• Cell volume: 2770 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0606
• Residual factor for significantly intense reflections: 0.0505
• Weighted residual factors for significantly intense reflections: 0.1374
• Weighted residual factors for all reflections included in the refinement: 0.1429
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No