Crystallography Open Database

Information card for entry 7019185

7019184 << 7019185 >> 7019186

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Coordinates	7019185.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C49.5 H72 Cl N2 P Pd
Calculated formula	C49.5 H72 Cl N2 P Pd
Title of publication	Generation of [(IPr)Pd(PR(2)Cl)] complexes via P-Cl reductive elimination.
Authors of publication	Tardiff, Bennett J.; Hesp, Kevin D.; Ferguson, Michael J.; Stradiotto, Mark
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	26
Pages of publication	7883 - 7885
a	21.4934 ± 0.0007 Å
b	13.5722 ± 0.0005 Å
c	31.6794 ± 0.0011 Å
α	90°
β	95.8069 ± 0.0004°
γ	90°
Cell volume	9193.9 ± 0.6 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0484
Residual factor for significantly intense reflections	0.0467
Weighted residual factors for significantly intense reflections	0.1252
Weighted residual factors for all reflections included in the refinement	0.1267
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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