Information card for entry 7019188

Structure parameters

• Formula: C37 H26 Cl2 Ni P2 S2
• Calculated formula: C37 H26 Cl2 Ni P2 S2
• Title of publication: Heteropolytopic phosphanylarylthiolato ligands: formation of cis isomers of nickel(ii), palladium(ii) and platinum(ii) complexes with 1-P(Biph)-2-SHC(6)H(4) (Biph = 1,1'-biphenyl-2,2'-diyl).
• Authors of publication: Hildebrand, Alexandra; Sárosi, Imola; Lönnecke, Peter; Silaghi-Dumitrescu, Luminiţa; Sárosi, Menyhárt B; Silaghi-Dumitrescu, Ioan; Hey-Hawkins, Evamarie
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 25
• Pages of publication: 7729 - 7736
• a: 13.65 ± 0.003 Å
• b: 18.542 ± 0.004 Å
• c: 13.989 ± 0.003 Å
• α: 90°
• β: 111.879 ± 0.004°
• γ: 90°
• Cell volume: 3285.6 ± 1.2 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0947
• Residual factor for significantly intense reflections: 0.0631
• Weighted residual factors for significantly intense reflections: 0.1362
• Weighted residual factors for all reflections included in the refinement: 0.1478
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No