Information card for entry 7019309

Structure parameters

• Formula: C34 H27 Cl5 N3 Sb
• Calculated formula: C34 H27 Cl5 N3 Sb
• SMILES: [Sb]1(Cl)(Cl)(Cl)[N]2c3c(CCc4nc(ccc4)CCc4c([N]1=C1C=2c2c5c(ccc2)cccc15)cccc4)cccc3.ClCCl
• Title of publication: Chemistry of the heavy group 15 elements with the pyridyl tethered 1,2-bis(imino)acenaphthene "clamshell" ligand.
• Authors of publication: Brazeau, Allison L.; Jones, Nathan D.; Ragogna, Paul J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 26
• Pages of publication: 7890 - 7896
• a: 10.222 ± 0.002 Å
• b: 11.568 ± 0.002 Å
• c: 14.686 ± 0.003 Å
• α: 101.08 ± 0.03°
• β: 91.95 ± 0.03°
• γ: 108.62 ± 0.03°
• Cell volume: 1606.5 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.044
• Residual factor for significantly intense reflections: 0.0346
• Weighted residual factors for significantly intense reflections: 0.0911
• Weighted residual factors for all reflections included in the refinement: 0.1158
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No