Crystallography Open Database

Information card for entry 7019664

7019663 << 7019664 >> 7019665

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Coordinates	7019664.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H42 Cu Mo8 N6 O33
Calculated formula	C29 H36 Cu Mo8 N6 O33
Title of publication	pH-dependent assembly of two inorganic-organic hybrid compounds based on octamolybdates: an unusual intercalated layer and a 3D 4-connected framework.
Authors of publication	Liu, Hai-Yan; Yang, Jin; Liu, Ying-Ying; Ma, Jian-Fang
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	33
Pages of publication	9922 - 9927
a	9.7092 ± 0.0002 Å
b	10.5053 ± 0.0002 Å
c	25.5093 ± 0.0004 Å
α	90°
β	99.26 ± 0.002°
γ	90°
Cell volume	2567.99 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0435
Residual factor for significantly intense reflections	0.0342
Weighted residual factors for significantly intense reflections	0.1027
Weighted residual factors for all reflections included in the refinement	0.1053
Goodness-of-fit parameter for all reflections included in the refinement	1.19
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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