Information card for entry 7019793

Structure parameters

• Formula: C73 H82 B2 Cl2 F20 P2
• Calculated formula: C73 H82 B2 Cl2 F20 P2
• Title of publication: Asymmetric hydrogenation of imines with a recyclable chiral frustrated Lewis pair catalyst.
• Authors of publication: Ghattas, Ghazi; Chen, Dianjun; Pan, Fangfang; Klankermayer, Jürgen
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 30
• Pages of publication: 9026 - 9028
• a: 15.07 ± 0.004 Å
• b: 13.208 ± 0.004 Å
• c: 17.862 ± 0.005 Å
• α: 90°
• β: 97.089 ± 0.008°
• γ: 90°
• Cell volume: 3528.2 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1082
• Residual factor for significantly intense reflections: 0.0699
• Weighted residual factors for significantly intense reflections: 0.1485
• Weighted residual factors for all reflections included in the refinement: 0.1736
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No