Information card for entry 7020197

Structure parameters

• Formula: C12 H50 Dy2 Ge2 N12 O2 Se6
• Calculated formula: C12 H38 Dy2 Ge2 N12 O2 Se6
• Title of publication: The first μ-Ge2Se8 ligand to lanthanide(III) centers: solvothermal syntheses and characterizations of lanthanide selenidogermanate complexes with a pentadentate polyamine as a co-ligand.
• Authors of publication: Chen, Ruihong; Tang, Weiwei; Liang, Jingjing; Jiang, Wenqing; Zhang, Yong; Jia, Dingxian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 40
• Pages of publication: 12439 - 12445
• a: 10.0259 ± 0.0019 Å
• b: 11.526 ± 0.002 Å
• c: 15.147 ± 0.003 Å
• α: 90°
• β: 99.03 ± 0.004°
• γ: 90°
• Cell volume: 1728.7 ± 0.6 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0409
• Weighted residual factors for significantly intense reflections: 0.0868
• Weighted residual factors for all reflections included in the refinement: 0.0901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No