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Information card for entry 7020226
Preview
Coordinates | 7020226.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C40.5 H64 Cl Ge P2 Rh |
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Calculated formula | C40.5 H64 Cl Ge P2 Rh |
Title of publication | Facile synthesis of rhodium and iridium complexes bearing a [PEP]-type ligand (E = Ge or Sn) via E-C bond cleavage. |
Authors of publication | Kameo, Hajime; Ishii, Sho; Nakazawa, Hiroshi |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2012 |
Journal volume | 41 |
Journal issue | 37 |
Pages of publication | 11386 - 11392 |
a | 14.955 ± 0.003 Å |
b | 14.07 ± 0.003 Å |
c | 19.454 ± 0.004 Å |
α | 90° |
β | 99.418 ± 0.003° |
γ | 90° |
Cell volume | 4038.3 ± 1.4 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0335 |
Residual factor for significantly intense reflections | 0.0306 |
Weighted residual factors for significantly intense reflections | 0.0706 |
Weighted residual factors for all reflections included in the refinement | 0.0719 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.118 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7020226.html
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