Information card for entry 7020251

Structure parameters

• Formula: C35 H38.11 Cl N5 O3.56 P Pd S
• Calculated formula: C35 H38.12 Cl N5 O3.56 P Pd S
• Title of publication: Mixed ligand palladium(ii) complexes of 6-methoxy-2-oxo-1,2-dihydroquinoline-3-carbaldehyde 4N-substituted thiosemicarbazones with triphenylphosphine co-ligand: Synthesis, crystal structure and biological properties.
• Authors of publication: Ramachandran, Eswaran; Senthil Raja, Duraisamy; Bhuvanesh, Nattamai S. P.; Natarajan, Karuppannan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 43
• Pages of publication: 13308 - 13323
• a: 13.11 ± 0.002 Å
• b: 12.08 ± 0.002 Å
• c: 24.071 ± 0.004 Å
• α: 90°
• β: 113.173 ± 0.011°
• γ: 90°
• Cell volume: 3504.5 ± 1 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0355
• Weighted residual factors for significantly intense reflections: 0.0895
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 1.014
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No