Information card for entry 7020355

Structure parameters

• Formula: C65 H62 B F24 N2 O2 P Pd
• Calculated formula: C65 H62 B F24 N2 O2 P Pd
• Title of publication: Migratory insertion reactions of nickel and palladium σ-alkyl complexes with a phosphinito-imine ligand.
• Authors of publication: Ortiz de la Tabla, Laura; Matas, Inmaculada; Alvarez, Eleuterio; Palma, Pilar; Cámpora, Juan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2012
• Journal volume: 41
• Journal issue: 48
• Pages of publication: 14524 - 14539
• a: 12.3365 ± 0.0009 Å
• b: 13.3092 ± 0.0011 Å
• c: 21.2562 ± 0.0018 Å
• α: 106.599 ± 0.004°
• β: 96.181 ± 0.004°
• γ: 92.774 ± 0.004°
• Cell volume: 3313.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0805
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1605
• Weighted residual factors for all reflections included in the refinement: 0.1719
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No