Information card for entry 7020804

Structure parameters

• Formula: C24 H48 Ni P2 S
• Calculated formula: C24 H48 Ni P2 S
• SMILES: [NiH](Sc1ccccc1)([P](C(C)C)(C(C)C)C(C)C)[P](C(C)C)(C(C)C)C(C)C
• Title of publication: Synthesis and chemistry of bis(triisopropylphosphine) nickel(i) and nickel(0) precursors.
• Authors of publication: Beck, Robert; Shoshani, Manar; Krasinkiewicz, Jonathan; Hatnean, Jillian A.; Johnson, Samuel A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 5
• Pages of publication: 1461 - 1475
• a: 9.1831 ± 0.0018 Å
• b: 11.038 ± 0.002 Å
• c: 13.734 ± 0.003 Å
• α: 81.49 ± 0.02°
• β: 88.23 ± 0.03°
• γ: 84.88 ± 0.03°
• Cell volume: 1371.1 ± 0.5 ų
• Cell temperature: 173.15 K
• Ambient diffraction temperature: 173.15 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.0951
• Weighted residual factors for all reflections included in the refinement: 0.1191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No