Information card for entry 7021044

Structure parameters

• Formula: C45 H37 F6 N5 Ni P3
• Calculated formula: C45 H37 F6 N5 Ni P3
• Title of publication: Synthesis and reactivity of nickel-hydride amino-bis-phosphinimine complexes.
• Authors of publication: Cariou, Renan; Graham, Todd W.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 12
• Pages of publication: 4237 - 4239
• a: 15.7941 ± 0.001 Å
• b: 18.9012 ± 0.0011 Å
• c: 28.6202 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8543.9 ± 0.9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 73
• Hermann-Mauguin space group symbol: I b c a
• Hall space group symbol: -I 2b 2c
• Residual factor for all reflections: 0.1086
• Residual factor for significantly intense reflections: 0.0637
• Weighted residual factors for significantly intense reflections: 0.1655
• Weighted residual factors for all reflections included in the refinement: 0.1979
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No