Information card for entry 7021114

Structure parameters

• Formula: C8 H8 Cl4 O2 W
• Calculated formula: C8 H8 Cl4 O2 W
• Title of publication: A crystallographic and spectroscopic study on the reactions of WCl6 with carbonyl compounds.
• Authors of publication: Dolci, Sara; Marchetti, Fabio; Pampaloni, Guido; Zacchini, Stefano
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 16
• Pages of publication: 5635 - 5648
• a: 20.19 ± 0.014 Å
• b: 7.212 ± 0.005 Å
• c: 8.608 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1253.4 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0345
• Weighted residual factors for significantly intense reflections: 0.0772
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No