Information card for entry 7021198

Structure parameters

• Formula: C24 H30 Ag2 Cl4 I2 N4
• Calculated formula: C24 H30 Ag2 Cl4 I2 N4
• Title of publication: Toward molecular rotors: tetra-N-heterocyclic carbene Ag(i)-halide cubane-type clusters.
• Authors of publication: Clark, Wesley D.; Tyson, Ginger E.; Hollis, T. Keith; Valle, Henry U.; Valente, Edward J.; Oliver, Allen G.; Dukes, Matthew P.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 20
• Pages of publication: 7338 - 7344
• a: 24.593 ± 0.019 Å
• b: 13.718 ± 0.01 Å
• c: 19.601 ± 0.015 Å
• α: 90°
• β: 102.384 ± 0.009°
• γ: 90°
• Cell volume: 6459 ± 8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0797
• Residual factor for significantly intense reflections: 0.0605
• Weighted residual factors for significantly intense reflections: 0.1276
• Weighted residual factors for all reflections included in the refinement: 0.1428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.16
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No