Information card for entry 7021229

Structure parameters

• Formula: C104 H100 Cl F18 N12 Ni2 O6 P3
• Calculated formula: C104 H100 Cl F18 N12 Ni2 O6 P3
• Title of publication: New ternary ligands consisting of an N4 bridging ligand and two terpyridines, and their Co(ii) and Ni(ii) dinuclear complexes. Structure, redox properties, and reaction with acid.
• Authors of publication: Kon, Hiroki; Nagata, Toshi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 16
• Pages of publication: 5697 - 5705
• a: 17.106 ± 0.003 Å
• b: 27.459 ± 0.004 Å
• c: 21.567 ± 0.003 Å
• α: 90°
• β: 101.727 ± 0.002°
• γ: 90°
• Cell volume: 9919 ± 3 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0625
• Residual factor for significantly intense reflections: 0.05
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1273
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No