Information card for entry 7021288

Structure parameters

• Formula: C72 H109 N6 Si6 U2
• Calculated formula: C63 H88 N6 Si6 U2
• Title of publication: A triamido-uranium(V) inverse-sandwich 10π-toluene tetraanion arene complex.
• Authors of publication: Patel, Dipti; Tuna, Floriana; McInnes, Eric J L; McMaster, Jonathan; Lewis, William; Blake, Alexander J; Liddle, Stephen T
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 15
• Pages of publication: 5224 - 5227
• a: 23.0405 ± 0.0003 Å
• b: 23.0405 ± 0.0003 Å
• c: 15.9177 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8450.14 ± 0.19 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 113
• Hermann-Mauguin space group symbol: P -4 21 m
• Hall space group symbol: P -4 2ab
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0724
• Weighted residual factors for significantly intense reflections: 0.19
• Weighted residual factors for all reflections included in the refinement: 0.1947
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No