Information card for entry 7021373

Structure parameters

• Formula: C88.5 H67 F40 N12 Pd Sn4
• Calculated formula: C88.5 H67 F40 N12 Pd Sn4
• SMILES: [Pd]([Sn]12N(CC[N]2(C)CCN1c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F)([Sn]12N(CC[N]2(C)CCN1c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F)([Sn]12N(CC[N]2(C)CCN1c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F)[Sn]12N(CC[N]2(C)CCN1c1c(c(c(c(c1F)F)F)F)F)c1c(c(c(c(c1F)F)F)F)F.c1(ccccc1)C.c1(ccccc1)C.c1(ccccc1)C.c1ccccc1
• Title of publication: Palladium complexes with stabilized germylene and stannylene ligands.
• Authors of publication: Kireenko, Marina M.; Zaitsev, Kirill V.; Oprunenko, Yuri F.; Churakov, Andrei V.; Tafeenko, Viktor A.; Karlov, Sergey S.; Zaitseva, Galina S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 22
• Pages of publication: 7901 - 7912
• a: 21.8677 ± 0.0016 Å
• b: 14.4922 ± 0.001 Å
• c: 58.575 ± 0.004 Å
• α: 90°
• β: 95.258 ± 0.001°
• γ: 90°
• Cell volume: 18485 ± 2 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1658
• Weighted residual factors for all reflections included in the refinement: 0.1761
• Goodness-of-fit parameter for all reflections included in the refinement: 1.149
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No