Information card for entry 7021433

Structure parameters

• Formula: C23 H20 Cl F12 O8 Pd2
• Calculated formula: C23 H20 Cl F12 O8 Pd2
• Title of publication: Axially chiral monomeric and dimeric square planar Pd(ii) complexes and their application to chiral tectonics.
• Authors of publication: Sato, Hisako; Morimoto, Kazuya; Mori, Yukie; Shinagawa, Yuji; Kitazawa, Takafumi; Yamagishi, Akihiko
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 21
• Pages of publication: 7579 - 7585
• a: 10.4812 ± 0.0006 Å
• b: 11.5797 ± 0.0006 Å
• c: 12.8934 ± 0.0007 Å
• α: 85.081 ± 0.001°
• β: 73.836 ± 0.001°
• γ: 86.555 ± 0.001°
• Cell volume: 1496.39 ± 0.14 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0634
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.0905
• Weighted residual factors for all reflections included in the refinement: 0.0966
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No