Information card for entry 7021499

Structure parameters

• Formula: C30 H55 B N P
• Calculated formula: C30 H55 B N P
• Title of publication: Boron azides in Staudinger oxidations and cycloadditions.
• Authors of publication: Melen, Rebecca L.; Lough, Alan J.; Stephan, Douglas W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 24
• Pages of publication: 8674 - 8683
• a: 10.639 ± 0.004 Å
• b: 20.992 ± 0.007 Å
• c: 22.501 ± 0.008 Å
• α: 63.106 ± 0.009°
• β: 80.088 ± 0.011°
• γ: 88.865 ± 0.01°
• Cell volume: 4405 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1058
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.1484
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No