Information card for entry 7021524

Structure parameters

• Formula: C24 H88 Fe N6 Nb9 O42.25
• Calculated formula: C24 H87 Fe1.007 N6 Nb8.993 O42.115
• Title of publication: Highly soluble iron- and nickel-substituted decaniobates with tetramethylammonium countercations.
• Authors of publication: Son, Jung-Ho; Ohlin, C André; Casey, William H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 21
• Pages of publication: 7529 - 7533
• a: 16.6125 ± 0.0014 Å
• b: 17.204 ± 0.0014 Å
• c: 24.08 ± 0.002 Å
• α: 90°
• β: 105.99 ± 0.001°
• γ: 90°
• Cell volume: 6615.8 ± 1 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0305
• Weighted residual factors for significantly intense reflections: 0.0692
• Weighted residual factors for all reflections included in the refinement: 0.0754
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No