Information card for entry 7021645

Structure parameters

• Common name: tris(trimethylphosphine)-(3,5-bis(trifluoromethyl) pyrazolate)cobalt(i)
• Chemical name: tris(trimethylphosphine)-(3,5-bis(trifluoromethyl) pyrazolate)cobalt(i)
• Formula: C14 H28 Co F6 N2 P3
• Calculated formula: C14 H28 Co F6 N2 P3
• Title of publication: Synthesis and structures of Co bis-trifluoromethylpyrazolate complexes.
• Authors of publication: Rivers, Joseph H.; Jones, Richard A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 12898 - 12907
• a: 9.2208 ± 0.0018 Å
• b: 16.675 ± 0.003 Å
• c: 15.634 ± 0.003 Å
• α: 90°
• β: 105.27 ± 0.03°
• γ: 90°
• Cell volume: 2319 ± 0.8 ų
• Cell temperature: 119 ± 2 K
• Ambient diffraction temperature: 119 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0921
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.104
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No