Crystallography Open Database

Information card for entry 7021694

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Coordinates	7021694.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C143 H108 F18 Lu2 N28 O18 S6
Calculated formula	C133 H97.5 F9 Lu2 N24.5 O9 S3
Title of publication	Monitoring helical twists and effective molarities in dinuclear triple-stranded lanthanide helicates.
Authors of publication	Ryan, Patrick E.; Guénée, Laure; Piguet, Claude
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	31
Pages of publication	11047 - 11055
a	18.3243 ± 0.0003 Å
b	23.0931 ± 0.0003 Å
c	23.8096 ± 0.0004 Å
α	90°
β	130.337 ± 0.001°
γ	90°
Cell volume	7680 ± 0.2 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	7
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0723
Residual factor for significantly intense reflections	0.0595
Weighted residual factors for significantly intense reflections	0.1831
Weighted residual factors for all reflections included in the refinement	0.1993
Goodness-of-fit parameter for all reflections included in the refinement	1.218
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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