Information card for entry 7021763

Structure parameters

• Formula: H56 Li6 O90 P2 W18
• Calculated formula: Li5.3 O89.85 P2 W18
• Title of publication: Quick and selective synthesis of Li6[α-P2W18O62]·28H2O soluble in various organic solvents.
• Authors of publication: Kato, Chisato; Nishihara, Sadafumi; Tsunashima, Ryo; Tatewaki, Yoko; Okada, Shuji; Ren, Xiao-Ming; Inoue, Katsuya; Long, De-Liang; Cronin, Leroy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 32
• Pages of publication: 11363 - 11366
• a: 15.1994 ± 0.0004 Å
• b: 15.1994 ± 0.0005 Å
• c: 56.421 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120 ± 0.007°
• Cell volume: 11288.2 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 166
• Hermann-Mauguin space group symbol: R -3 m :H
• Hall space group symbol: -R 3 2"
• Residual factor for all reflections: 0.0186
• Residual factor for significantly intense reflections: 0.0158
• Weighted residual factors for significantly intense reflections: 0.0358
• Weighted residual factors for all reflections included in the refinement: 0.0374
• Goodness-of-fit parameter for all reflections included in the refinement: 0.999
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No