Information card for entry 7021768

Structure parameters

• Formula: C27 H34 B O3 Ru2
• Calculated formula: C26.963 H34 B O3 Ru2
• Title of publication: A fine tuning of metallaborane to bridged-boryl complex, [(Cp*Ru)2(μ-H)(μ-CO)(μ-Bcat)] (cat = 1,2-O2C6H4; Cp* = η(5)-C5Me5).
• Authors of publication: Anju, R. S.; Roy, Dipak Kumar; Geetharani, K.; Mondal, Bijan; Varghese, Babu; Ghosh, Sundargopal
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 36
• Pages of publication: 12828 - 12831
• a: 10.773 ± 0.004 Å
• b: 10.793 ± 0.004 Å
• c: 12.098 ± 0.004 Å
• α: 73.97 ± 0.02°
• β: 73.995 ± 0.019°
• γ: 83.093 ± 0.019°
• Cell volume: 1298.1 ± 0.8 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1759
• Residual factor for significantly intense reflections: 0.0694
• Weighted residual factors for significantly intense reflections: 0.129
• Weighted residual factors for all reflections included in the refinement: 0.1827
• Goodness-of-fit parameter for all reflections included in the refinement: 1.133
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No