Information card for entry 7021853

Structure parameters

• Common name: tetramethylammonium decaniobomanganate
• Formula: C32 H101 Mn N8 Nb10 O54
• Calculated formula: C32 H101 Mn N8 Nb10 O54.134
• Title of publication: A decatungstate-type polyoxoniobate with centered manganese: [H2Mn(IV)Nb10O32](8-) as a soluble tetramethylammonium salt.
• Authors of publication: Son, Jung-Ho; Casey, William H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 37
• Pages of publication: 13339 - 13342
• a: 13.9537 ± 0.0006 Å
• b: 34.0884 ± 0.0014 Å
• c: 18.0134 ± 0.0007 Å
• α: 90°
• β: 92.907 ± 0.001°
• γ: 90°
• Cell volume: 8557.2 ± 0.6 ų
• Cell temperature: 88 ± 2 K
• Ambient diffraction temperature: 88 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0481
• Residual factor for significantly intense reflections: 0.0364
• Weighted residual factors for significantly intense reflections: 0.0867
• Weighted residual factors for all reflections included in the refinement: 0.0937
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No