Information card for entry 7021855

Structure parameters

• Chemical name: trans-tetrafluoridobis(triphenylphosphane oxide-O)silicon(IV)
• Formula: C36 H30 F4 O2 P2 Si
• Calculated formula: C36 H30 F4 O2 P2 Si
• Title of publication: Hypervalent neutral O-donor ligand complexes of silicon tetrafluoride, comparisons with other group 14 tetrafluorides and a search for soft donor ligand complexes.
• Authors of publication: George, Kathryn; Hector, Andrew L.; Levason, William; Reid, Gillian; Sanderson, George; Webster, Michael; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 7
• Pages of publication: 1584 - 1593
• a: 12.6885 ± 0.0015 Å
• b: 13.7509 ± 0.0015 Å
• c: 14.869 ± 0.002 Å
• α: 62.564 ± 0.006°
• β: 82.697 ± 0.006°
• γ: 80.305 ± 0.006°
• Cell volume: 2266 ± 0.5 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.149
• Residual factor for significantly intense reflections: 0.0822
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1592
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No