Information card for entry 7021857

Structure parameters

• Chemical name: tetrafluoro(bis(diphenylphosphino)methane dioxide)germanium(IV) dichloromethane solvate
• Formula: C26 H24 Cl2 F4 Ge O2 P2
• Calculated formula: C26 H24 Cl2 F4 Ge O2 P2
• Title of publication: Hypervalent neutral O-donor ligand complexes of silicon tetrafluoride, comparisons with other group 14 tetrafluorides and a search for soft donor ligand complexes.
• Authors of publication: George, Kathryn; Hector, Andrew L.; Levason, William; Reid, Gillian; Sanderson, George; Webster, Michael; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 7
• Pages of publication: 1584 - 1593
• a: 12.87 ± 0.003 Å
• b: 13.779 ± 0.003 Å
• c: 15.83 ± 0.003 Å
• α: 90°
• β: 92.748 ± 0.012°
• γ: 90°
• Cell volume: 2804 ± 1 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.154
• Residual factor for significantly intense reflections: 0.0963
• Weighted residual factors for significantly intense reflections: 0.1607
• Weighted residual factors for all reflections included in the refinement: 0.1861
• Goodness-of-fit parameter for all reflections included in the refinement: 1.116
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No