Information card for entry 7021866

Structure parameters

• Formula: C24 H20 N8 Pd2
• Calculated formula: C24 H20 N8 Pd2
• Title of publication: New cyclometallated precursors of unsubstituted N-phenylpyrazole [{Pd(phpz)(μ-X)}2] (X = AcO or OH) and study of their reactivity towards selected ligands.
• Authors of publication: Serrano, José Luis; García, Luis; Pérez, José; Pérez, Eduardo; Galiana, José Miguel; García, Joaquín; Martínez, Marina; Sánchez, Gregorio; da Silva, Ivan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2011
• Journal volume: 40
• Journal issue: 1
• Pages of publication: 156 - 168
• a: 23.3603 ± 0.0005 Å
• b: 8.95252 ± 0.00017 Å
• c: 11.5684 ± 0.0002 Å
• α: 90°
• β: 104.074 ± 0.0014°
• γ: 90°
• Cell volume: 2346.72 ± 0.08 ų
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor R(I) for significantly intense reflections: 8.0273
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 0.824 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No