Information card for entry 7021868

Structure parameters

• Formula: C125 H109 Cl6 Dy5 N4 O25
• Calculated formula: C123 H105 Cl2 Dy5 N4 O25
• Title of publication: Slow magnetic relaxation in four square-based pyramidal dysprosium hydroxo clusters ligated by chiral amino acid anions - a comparative study.
• Authors of publication: Thielemann, Dominique T.; Wagner, Anna T.; Lan, Yanhua; Anson, Christopher E.; Gamer, Michael T.; Powell, Annie K.; Roesky, Peter W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 41
• Pages of publication: 14794 - 14800
• a: 18.2305 ± 0.0005 Å
• b: 18.9609 ± 0.0004 Å
• c: 33.7647 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11671.3 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0352
• Residual factor for significantly intense reflections: 0.0287
• Weighted residual factors for significantly intense reflections: 0.0603
• Weighted residual factors for all reflections included in the refinement: 0.0619
• Goodness-of-fit parameter for all reflections included in the refinement: 0.951
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No