Information card for entry 7022012

Structure parameters

• Formula: C66 H70 Cl2 N2 O3 P4 Pd2 Te2
• Calculated formula: C66 H64 Cl2 N2 O3 P4 Pd2 Te2
• Title of publication: Reactivity of 2-chalcogenopyridines with palladium-phosphine complexes: isolation of different complexes depending on the nature of chalcogen atom and phosphine ligand.
• Authors of publication: Chauhan, Rohit Singh; Kedarnath, G.; Wadawale, Amey; Slawin, Alexandra M. Z.; Jain, Vimal K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 1
• Pages of publication: 259 - 269
• a: 11.934 ± 0.006 Å
• b: 13.083 ± 0.007 Å
• c: 13.46 ± 0.007 Å
• α: 114.084 ± 0.002°
• β: 99.385 ± 0.004°
• γ: 111.686 ± 0.005°
• Cell volume: 1656.3 ± 1.5 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0945
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1577
• Weighted residual factors for all reflections included in the refinement: 0.1727
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No