Information card for entry 7022015

Structure parameters

• Formula: C168 H162 Cl21 P12 Pd6 Te4
• Calculated formula: C168 H162 Cl21 P12 Pd6 Te4
• Title of publication: Reactivity of 2-chalcogenopyridines with palladium-phosphine complexes: isolation of different complexes depending on the nature of chalcogen atom and phosphine ligand.
• Authors of publication: Chauhan, Rohit Singh; Kedarnath, G.; Wadawale, Amey; Slawin, Alexandra M. Z.; Jain, Vimal K.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 1
• Pages of publication: 259 - 269
• a: 14.2448 ± 0.0004 Å
• b: 18.8456 ± 0.0006 Å
• c: 18.9875 ± 0.0005 Å
• α: 81.392 ± 0.002°
• β: 83.613 ± 0.002°
• γ: 69.894 ± 0.003°
• Cell volume: 4722.9 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1837
• Residual factor for significantly intense reflections: 0.0958
• Weighted residual factors for significantly intense reflections: 0.1997
• Weighted residual factors for all reflections included in the refinement: 0.2258
• Goodness-of-fit parameter for all reflections included in the refinement: 1.177
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No