Information card for entry 7022618

Structure parameters

• Common name: compound 9
• Formula: C52 H46 Cl4 O5 Ru3 Si3
• Calculated formula: C52 H46 Cl4 O5 Ru3 Si3
• Title of publication: Coupling of acetylene molecules on ruthenium clusters, involving cleavage of C-Si bonds in the alkyne and coordination of a phenyl ring of a SiPh3 group.
• Authors of publication: González-López, Vianney; Leyva, Marco A.; Rosales-Hoz, María J
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 15
• Pages of publication: 5401 - 5411
• a: 9.9128 ± 0.0002 Å
• b: 15.4684 ± 0.0004 Å
• c: 17.7928 ± 0.0004 Å
• α: 72.928 ± 0.002°
• β: 84.899 ± 0.001°
• γ: 86.614 ± 0.001°
• Cell volume: 2596.16 ± 0.11 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1086
• Residual factor for significantly intense reflections: 0.0606
• Weighted residual factors for significantly intense reflections: 0.1512
• Weighted residual factors for all reflections included in the refinement: 0.1784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No