Information card for entry 7022623

Structure parameters

• Formula: C58 H48 Cl2 F6 N O7 P3 Pt S2 Si
• Calculated formula: C58 H46 Cl2 F6 N O7 P3 Pt S2 Si
• Title of publication: Heterolytic activation of dihydrogen by platinum and palladium complexes.
• Authors of publication: Leñero, Karina Q Almeida; Guari, Yannick; Kamer, Paul C. J.; van Leeuwen, Piet W. N. M.; Donnadieu, Bruno; Sabo-Etienne, Sylviane; Chaudret, Bruno; Lutz, Martin; Spek, Anthony L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 18
• Pages of publication: 6495 - 6512
• a: 23.757 ± 0.005 Å
• b: 13.009 ± 0.003 Å
• c: 38.06 ± 0.008 Å
• α: 90°
• β: 91.27 ± 0.03°
• γ: 90°
• Cell volume: 11760 ± 4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 K
• Number of distinct elements: 10
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0473
• Residual factor for significantly intense reflections: 0.0395
• Weighted residual factors for significantly intense reflections: 0.0958
• Weighted residual factors for all reflections included in the refinement: 0.1015
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No