Information card for entry 7022765

Structure parameters

• Chemical name: bis(nitrato-O,O')-1,4,7,10,13-pentaoxacyclopentadecane-lead(II)
• Formula: C10 H20 N2 O11 Pb
• Calculated formula: C10 H20 N2 O11 Pb
• SMILES: [Pb]123456([O]7CC[O]1CC[O]2CC[O]3CC[O]4CC7)(ON(=[O]5)=O)ON(=[O]6)=O
• Title of publication: Lead(II) tetrafluoroborate and hexafluorophosphate complexes with crown ethers, mixed O/S- and O/Se-donor macrocycles and unusual [BF(4)](-) and [PF(6)](-) coordination.
• Authors of publication: Farina, Paolo; Latter, Thomas; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 13
• Pages of publication: 4714 - 4724
• a: 15.307 ± 0.004 Å
• b: 8.303 ± 0.002 Å
• c: 13.152 ± 0.004 Å
• α: 90°
• β: 92.815 ± 0.004°
• γ: 90°
• Cell volume: 1669.5 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0342
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for significantly intense reflections: 0.071
• Weighted residual factors for all reflections included in the refinement: 0.0727
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No