Information card for entry 7022768

Structure parameters

• Chemical name: bis(1,4,7-trioxa-10,13-dithiacyclopentadecane)lead(II) tetrafluoroborate dichloromethane solvate
• Formula: C21.22 H42.44 B2 Cl2.44 F8 O6 Pb S4
• Calculated formula: C21 H40 B2 Cl2.44 F8 O6 Pb S4
• Title of publication: Lead(II) tetrafluoroborate and hexafluorophosphate complexes with crown ethers, mixed O/S- and O/Se-donor macrocycles and unusual [BF(4)](-) and [PF(6)](-) coordination.
• Authors of publication: Farina, Paolo; Latter, Thomas; Levason, William; Reid, Gillian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 13
• Pages of publication: 4714 - 4724
• a: 18.747 ± 0.003 Å
• b: 28.254 ± 0.01 Å
• c: 13.263 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7025 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 56
• Hermann-Mauguin space group symbol: P c c n
• Hall space group symbol: -P 2ab 2ac
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.0957
• Weighted residual factors for all reflections included in the refinement: 0.1068
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No