Information card for entry 7023201

Structure parameters

• Formula: C200 H208 Cu10 Fe4 I10 O32 P8
• Calculated formula: C200 H208 Cu10 Fe4 I10 O32 P8
• Title of publication: Synthesis, transition metal chemistry and catalytic reactions of ferrocenylbis(phosphonite), [Fe{C5H4P(OC6H3(OMe-o)(C3H5-p))2}2].
• Authors of publication: Rao, Sowmya; Mague, Joel T.; Balakrishna, Maravanji S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 32
• Pages of publication: 11695 - 11708
• a: 14.6299 ± 0.0014 Å
• b: 16.1611 ± 0.0015 Å
• c: 24.111 ± 0.002 Å
• α: 71.67 ± 0.001°
• β: 80.188 ± 0.001°
• γ: 71.003 ± 0.001°
• Cell volume: 5102 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1275
• Residual factor for significantly intense reflections: 0.0649
• Weighted residual factors for significantly intense reflections: 0.1437
• Weighted residual factors for all reflections included in the refinement: 0.172
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No