Crystallography Open Database

Information card for entry 7023917

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Coordinates	7023917.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Ag3 H55 O105 Pr4 Si2 W22
Calculated formula	Ag3 O102 Pr4 Si2 W22
Title of publication	Monolacunary Keggin polyoxometalates connected to ten 4d or 4f metal atoms.
Authors of publication	Pang, Haijun; Gómez-García, Carlos J; Peng, Jun; Ma, Huiyuan; Zhang, Chunjing; Wu, Qingyin
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	47
Pages of publication	16596 - 16601
a	12.343 ± 0.005 Å
b	13.215 ± 0.005 Å
c	18.025 ± 0.005 Å
α	94.681 ± 0.005°
β	92.263 ± 0.005°
γ	105.038 ± 0.005°
Cell volume	2824.3 ± 1.8 Å³
Cell temperature	571 ± 2 K
Ambient diffraction temperature	571 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1197
Residual factor for significantly intense reflections	0.0556
Weighted residual factors for significantly intense reflections	0.0767
Weighted residual factors for all reflections included in the refinement	0.0811
Goodness-of-fit parameter for all reflections included in the refinement	1.006
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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