Information card for entry 7024018

Structure parameters

• Chemical name: mu3-[N,N',N''-Tris(methyltrifluoroacetylmethylmethylidene) trimesoyltrihydrazine hexa(pyridine)tricopper(2+) pyridine solvate
• Formula: C61.5 H54.5 Cu3 F9 N13.5 O7
• Calculated formula: C61.5 H52.5 Cu3 F9 N13.5 O7
• Title of publication: Spacer-armed copper(ii) complexes with benzenecarboxylic acids and trifluoroacetylacetone aroylhydrazones.
• Authors of publication: Shul'gin, Victor F.; Konnik, Oleg V.; Gusev, Alexey N.; Boča, Roman; Dlháň, Lubor; Rusanov, Eduard B.; Alexandrov, Grygory G.; Eremenko, Igor L.; Linert, Wolfgang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2013
• Journal volume: 42
• Journal issue: 48
• Pages of publication: 16878 - 16886
• a: 12.6441 ± 0.0004 Å
• b: 18.1616 ± 0.0006 Å
• c: 18.3761 ± 0.0006 Å
• α: 118.943 ± 0.001°
• β: 107.308 ± 0.001°
• γ: 90.689 ± 0.001°
• Cell volume: 3463.6 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1163
• Residual factor for significantly intense reflections: 0.0754
• Weighted residual factors for significantly intense reflections: 0.212
• Weighted residual factors for all reflections included in the refinement: 0.2532
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No