Information card for entry 7024025

Structure parameters

• Formula: C48 H81 Fe9 N16 Na9 O123 Si3 W28
• Calculated formula: C30 H58 Fe9 N10 Na5 O123 Si3 W28
• Title of publication: Preparation of polyoxometalates in ionic liquids by ionothermal synthesis.
• Authors of publication: Lin, Shiwei; Liu, Wenli; Li, Yangguang; Wu, Qiong; Wang, Enbo; Zhang, Zhiming
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 7
• Pages of publication: 1740 - 1744
• a: 15.302 ± 0.003 Å
• b: 23.309 ± 0.005 Å
• c: 27.828 ± 0.006 Å
• α: 86.25 ± 0.03°
• β: 89.04 ± 0.03°
• γ: 89.28 ± 0.03°
• Cell volume: 9902 ± 4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1575
• Residual factor for significantly intense reflections: 0.0857
• Weighted residual factors for significantly intense reflections: 0.1799
• Weighted residual factors for all reflections included in the refinement: 0.2132
• Goodness-of-fit parameter for all reflections included in the refinement: 0.937
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No