Information card for entry 7024091

Structure parameters

• Formula: C12 H76 Cs8 O106 Si2 Sn6 W18
• Calculated formula: C12 H10 Cs7.5 O106 Si2 Sn6 W18
• Title of publication: Trilacunary A-beta-Keggin tungstogermanates and -silicates functionalized with phenyltin(IV) electrophiles.
• Authors of publication: Reinoso, Santiago; Piedra-Garza, Luis Fernando; Dickman, Michael H.; Praetorius, Antonia; Biesemans, Monique; Willem, Rudolph; Kortz, Ulrich
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 248 - 255
• a: 13.3563 ± 0.0013 Å
• b: 18.997 ± 0.002 Å
• c: 23.492 ± 0.002 Å
• α: 97.12 ± 0.004°
• β: 94.802 ± 0.004°
• γ: 96.02 ± 0.004°
• Cell volume: 5853.7 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.0499
• Weighted residual factors for significantly intense reflections: 0.1157
• Weighted residual factors for all reflections included in the refinement: 0.1333
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No