Information card for entry 7024099

Structure parameters

• Common name: chloro(N,N,N',N'',N''-pentamethyl- diethylenetriamine)germanium(ii) trichlorogermanate(ii)
• Chemical name: chloro(N,N,N',N",N"-pentamethyl-diethylenetriamine)germanium(II) trichlorogermanate(II)
• Formula: C9 H23 Cl4 Ge2 N3
• Calculated formula: C9 H23 Cl4 Ge2 N3
• SMILES: [Ge]12(Cl)[N](C)(C)CC[N]1(C)CC[N]2(C)C.[Ge](Cl)(Cl)[Cl-]
• Title of publication: Synthesis and structural characterisation of germanium(II) halide complexes with neutral N-donor ligands.
• Authors of publication: Cheng, Fei; Dyke, John M.; Ferrante, Francesco; Hector, Andrew L.; Levason, William; Reid, Gillian; Webster, Michael; Zhang, Wenjian
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 3
• Pages of publication: 847 - 856
• a: 6.3451 ± 0.001 Å
• b: 11.813 ± 0.002 Å
• c: 13.166 ± 0.003 Å
• α: 112.008 ± 0.01°
• β: 98.953 ± 0.01°
• γ: 93.393 ± 0.015°
• Cell volume: 896.3 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0943
• Residual factor for significantly intense reflections: 0.0602
• Weighted residual factors for significantly intense reflections: 0.1141
• Weighted residual factors for all reflections included in the refinement: 0.1328
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No