Information card for entry 7024136

Structure parameters

• Common name: (K(2,2,2-crypt))4(Cu2(As7)2)*2en
• Chemical name: [K(2,2,2-crypt)]4[Cu2(As7)2]*2en
• Formula: C76 H160 As14 Cu2 K4 N12 O24
• Calculated formula: C76 H160.04 As14 Cu2 K4 N12 O24
• Title of publication: Reactivity studies of group 15 Zintl ions towards homoleptic post-transition metal organometallics: a 'bottom-up' approach to bimetallic molecular clusters.
• Authors of publication: Knapp, Caroline; Zhou, Binbin; Denning, Mark S.; Rees, Nicholas H.; Goicoechea, Jose M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 2
• Pages of publication: 426 - 436
• a: 15.154 ± 0.0002 Å
• b: 15.181 ± 0.0002 Å
• c: 15.764 ± 0.0002 Å
• α: 111.46 ± 0.001°
• β: 90.07 ± 0.001°
• γ: 118.9 ± 0.001°
• Cell volume: 2883.41 ± 0.08 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.1318
• Weighted residual factors for all reflections included in the refinement: 0.1372
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No